Electron imaging of dielectrics under simultaneous electron–ion irradiation
نویسندگان
چکیده
We demonstrate that if charging caused by electron irradiation of an insulator is controlled by a defocused flux of soft-landing positive ions, secondary electron ~SE! images can contain contrast due to lateral variations in ~i! changes in the SE yield caused by subsurface trapped charge and ~ii! the SE-ion recombination rate. Both contrast mechanisms can provide information on microscopic variations in dielectric properties. We present a model of SE contrast formation that accounts for localized charging and the effects of gas ions on the SE emission process, emitted electrons above the sample surface, and subsurface trapped charge. The model explains the ion flux dependence of charge-induced SE contrast, an increase in the sensitivity to surface contrast observed in SE images of charged dielectrics, and yields procedures for identification of contrast produced by localized sample charging. © 2002 American Institute of Physics. @DOI: 10.1063/1.1448875#
منابع مشابه
In-situ observation and atomic resolution imaging of the ion irradiation induced amorphisation of graphene
Ion irradiation has been observed to induce a macroscopic flattening and in-plane shrinkage of graphene sheets without a complete loss of crystallinity. Electron diffraction studies performed during simultaneous in-situ ion irradiation have allowed identification of the fluence at which the graphene sheet loses long-range order. This approach has facilitated complementary ex-situ investigations...
متن کاملElectric fields produced by electron irradiation of insulators in a low vacuum environment
We report on the properties of electric fields generated as a result of electron irradiation of dielectrics in a low vacuum scanning electron microscope. Individual field components produced by ~i! ionized gas molecules located outside the sample surface and ~ii! subsurface trapped charge were detected by measurements of changes in ~i! primary electron landing energy and ~ii! secondary electron...
متن کاملMeV ion-induced strain at nanoisland-semiconductor surface and interfaces
Strain at surfaces and interfaces play an important role in the optical and electronic properties of materials. MeV ion-induced strain determination in single crystal silicon substrates and in Ag (nanoisland)/Si(111) at surface and interfaces has been carried out using transmission electron microscopy (TEM) and surface-sensitive X-ray diffraction. Ag nanoislands are grown under various surface ...
متن کاملIn situ TEM of radiation effects in complex ceramics.
In situ transmission electron microscopy (TEM) has been extensively applied to study radiation effects in a wide variety of materials, such as metals, ceramics and semiconductors and is an indispensable tool in obtaining a fundamental understanding of energetic beam-matter interactions, damage events, and materials' behavior under intense radiation environments. In this article, in situ TEM obs...
متن کاملApplication of Electron Beam/MnII Process for Humic Acid Removal from Aqueous Solutions
Introduction: Natural organic matters (NOMs) existing in water resources led to various problems such as formation of disinfectant by-products (DBPs). Humic matters like humic acid (HA) are component of NOMs that should be removed from water. Advanced oxidation process (AOPs) is one of the NOMs removal methods. The aim of this study was to survey the degradation of humic acid by electron beam i...
متن کاملذخیره در منابع من
با ذخیره ی این منبع در منابع من، دسترسی به آن را برای استفاده های بعدی آسان تر کنید
عنوان ژورنال:
دوره شماره
صفحات -
تاریخ انتشار 2002